5GKG
Structure of EndoMS-dsDNA1'' complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-05-23 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.9800 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 92.420, 92.420, 405.080 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 24.810 - 2.600 |
R-factor | 0.171 |
Rwork | 0.168 |
R-free | 0.23100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5BSL |
RMSD bond length | 0.010 |
RMSD bond angle | 1.316 |
Data reduction software | MOSFLM |
Data scaling software | MOSFLM |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.740 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 30062 | |
<I/σ(I)> | 22.3 | 9.4 |
Completeness [%] | 91.7 | 88.9 |
Redundancy | 1.8 | 1.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 291 | CALCIUM ACETATE, SODIUM CACODYLATE, PEG8000, GLYCEROL |