5GID
Crystal structure of VDR in complex with DLAM-4 (C2 form)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 90 |
Detector technology | CCD |
Collection date | 2014-06-14 |
Detector | MAR CCD 130 mm |
Wavelength(s) | 1.0000 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 154.510, 42.345, 42.320 |
Unit cell angles | 90.00, 96.46, 90.00 |
Refinement procedure
Resolution | 40.821 - 2.151 |
R-factor | 0.202 |
Rwork | 0.199 |
R-free | 0.23330 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.879 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | MOLREP |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 41.000 |
High resolution limit [Å] | 2.150 |
Number of reflections | 14860 |
<I/σ(I)> | 13.33 |
Completeness [%] | 99.0 |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1M Tris-HCl, PEG 8000, NaCl |