5G55
3-Quinoline Carboxamides inhibitors of Pi3K
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF |
Synchrotron site | ESRF |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Wavelength(s) | 0.9330 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 140.077, 67.182, 104.559 |
Unit cell angles | 90.00, 96.65, 90.00 |
Refinement procedure
Resolution | 72.000 - 2.450 |
Rwork | 0.254 |
R-free | 0.32206 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.012 |
RMSD bond angle | 1.680 |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 70.000 |
High resolution limit [Å] | 2.450 |
Rmerge | 0.060 |
Number of reflections | 32672 |
Completeness [%] | 96.0 |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |