5G0X
Pseudomonas aeruginosa HDAH bound to acetate.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-04-03 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 81.390, 81.390, 205.850 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 75.690 - 1.700 |
| R-factor | 0.13677 |
| Rwork | 0.134 |
| R-free | 0.18403 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1zz0 |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.508 |
| Data reduction software | MOSFLM |
| Data scaling software | Aimless |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 75.690 | 1.730 |
| High resolution limit [Å] | 1.700 | 1.700 |
| Rmerge | 0.280 | 1.090 |
| Number of reflections | 77011 | |
| <I/σ(I)> | 5.9 | 2.4 |
| Completeness [%] | 100.0 | 97.7 |
| Redundancy | 11.5 | 11.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | pH 7.5 |
