5FYV
Crystal structure of the catalytic domain of human JARID1B in complex with oxaloacetate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-05-20 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 142.180, 142.180, 152.150 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 57.071 - 1.870 |
R-factor | 0.1993 |
Rwork | 0.198 |
R-free | 0.23000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5a3p |
RMSD bond length | 0.008 |
RMSD bond angle | 1.090 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | DIMPLE |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 71.090 | 1.920 |
High resolution limit [Å] | 1.870 | 1.870 |
Rmerge | 0.080 | 1.500 |
Number of reflections | 75124 | |
<I/σ(I)> | 23 | 1.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 19.8 | 19.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 0.1M HEPES PH 7.5 -- 0.8M POTASSIUM PHOSPHATE DIBASIC -- 0.8M SODIUM PHOSPHATE MONOBASIC |