5FRC
Structure of urate oxidase prepared by the 'soak-and-freeze' method under 42 bar of oxygen pressure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 80.898, 95.351, 104.672 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.675 - 1.443 |
R-factor | 0.1427 |
Rwork | 0.141 |
R-free | 0.16480 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4po6 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.072 |
Data reduction software | XDS |
Data scaling software | XDS (XSCALE) |
Phasing software | MOLREP |
Refinement software | PHENIX ((PHENIX.REFINE: 1.9_1692)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.680 | 1.530 |
High resolution limit [Å] | 1.440 | 1.440 |
Rmerge | 0.060 | 0.060 |
Number of reflections | 70982 | |
<I/σ(I)> | 11.5 | 1.5 |
Completeness [%] | 97.5 | 94 |
Redundancy | 4.2 | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |