5FR1
Double acetylated RhoGDI-alpha in complex with RhoA-GDP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-08-12 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 53.100, 67.640, 120.230 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 60.110 - 2.750 |
R-factor | 0.20173 |
Rwork | 0.199 |
R-free | 0.25598 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1hh4 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.674 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.110 | 2.900 |
High resolution limit [Å] | 2.750 | 2.750 |
Rmerge | 0.097 | 0.364 |
Number of reflections | 11805 | |
<I/σ(I)> | 9.2 | 3 |
Completeness [%] | 99.8 | 98.7 |
Redundancy | 3.7 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.5 | 4 M SODIUM FORMATE, 0.1 M SODIUM ACETATE PH 4.5 |