5FBL
PI4KB in complex with Rab11 and the MI356 Inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-05-29 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9796 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 49.484, 104.902, 188.022 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.005 - 3.372 |
R-factor | 0.2441 |
Rwork | 0.243 |
R-free | 0.26880 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4d0l |
RMSD bond length | 0.004 |
RMSD bond angle | 1.013 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.010 | 3.490 |
High resolution limit [Å] | 3.370 | 3.370 |
Rmerge | 0.113 | |
Total number of observations | 55513 | |
Number of reflections | 14419 | |
<I/σ(I)> | 14.11 | |
Completeness [%] | 99.5 | 97.19 |
Redundancy | 3.85 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 1M Lithium chloride, 0.1M Citric acid pH=5, 10% (w/v) PEG 6000 |