5EK7
Structure of the autoinhibited Epha2 JMS-KD
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL13B1 |
Synchrotron site | NSRRC |
Beamline | BL13B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-11-27 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 63.475, 75.242, 80.483 |
Unit cell angles | 90.00, 112.67, 90.00 |
Refinement procedure
Resolution | 26.806 - 1.901 |
R-factor | 0.1725 |
Rwork | 0.171 |
R-free | 0.20510 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.146 |
Data reduction software | SCALEPACK |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.2_1309) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 30.000 | 30.000 | 1.970 |
High resolution limit [Å] | 1.900 | 4.090 | 1.900 |
Rmerge | 0.060 | 0.045 | 0.304 |
Rmeas | 0.071 | 0.054 | 0.359 |
Rpim | 0.038 | 0.029 | 0.189 |
Total number of observations | 198736 | ||
Number of reflections | 54658 | ||
<I/σ(I)> | 12.6 | ||
Completeness [%] | 99.7 | 99.4 | 99.7 |
Redundancy | 3.6 | 3.5 | 3.5 |
CC(1/2) | 0.994 | 0.901 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 4% Tacsimate, 5%(w/v) PEG3350, 5% 2-propanol |