5EJW
Crystal structure of chromobox homolog 7 (CBX7) chromodomain with MS351
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X6A |
Synchrotron site | NSLS |
Beamline | X6A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-05-02 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 52.748, 52.748, 76.813 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.410 - 2.600 |
R-factor | 0.19642 |
Rwork | 0.195 |
R-free | 0.23707 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1pdq |
RMSD bond length | 0.016 |
RMSD bond angle | 1.749 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | BALBES |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.200 | 2.640 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.099 | 0.593 |
Number of reflections | 4105 | |
<I/σ(I)> | 29.2 | 5.2 |
Completeness [%] | 99.8 | 97.7 |
Redundancy | 12.8 | 13 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 290 | 0.1M Tris 8.5, 2.0M Ammonium Sulfate |