5E3A
Structure of human DPP3 in complex with opioid peptide leu-enkephalin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-04-20 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.972390 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 119.558, 105.757, 64.992 |
Unit cell angles | 90.00, 93.43, 90.00 |
Refinement procedure
Resolution | 39.576 - 2.050 |
R-factor | 0.2113 |
Rwork | 0.209 |
R-free | 0.25990 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3t6b |
RMSD bond length | 0.002 |
RMSD bond angle | 0.616 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHENIX (1.9_1692) |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.580 | 2.121 |
High resolution limit [Å] | 2.050 | 2.050 |
Rmerge | 0.089 | 0.620 |
Number of reflections | 48267 | |
<I/σ(I)> | 10.73 | 1.85 |
Completeness [%] | 95.1 | 95.45 |
Redundancy | 3 | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.2 | 293 | 0.056M SODIUM PHOSPHATE MONOBASIC MONOHYDRATE, 1.344M POTASSIUM PHOSPHATE DIBASIC |