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5DJ8

Fc Heterodimer Design 7.7 D399M/Y407A + T366V/K409I

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 31-ID
Synchrotron siteAPS
Beamline31-ID
Temperature [K]193
Detector technologyCCD
Collection date2013-10-02
DetectorRAYONIX MX-225
Wavelength(s)0.97931
Spacegroup nameP 1 21 1
Unit cell lengths60.508, 67.669, 78.376
Unit cell angles90.00, 104.34, 90.00
Refinement procedure
Resolution28.800 - 2.400
R-factor0.21674
Rwork0.214
R-free0.26025
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.010
RMSD bond angle1.518
Data scaling softwareSCALA (3.3.20)
Phasing softwareMOLREP
Refinement softwareREFMAC (5.7.0017)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]28.80067.6692.530
High resolution limit [Å]2.4007.5902.400
Rmerge0.0470.455
Rmeas0.121
Rpim0.0640.0300.315
Total number of observations82649263610554
Number of reflections23694
<I/σ(I)>7.314.22.4
Completeness [%]98.094.296.4
Redundancy3.53.53.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION29431% PEG 3350 + 100mM Ammonium Iodide

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