5DFF
Human APE1 product complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-11-22 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 |
Unit cell lengths | 44.514, 61.716, 72.053 |
Unit cell angles | 83.89, 78.81, 88.00 |
Refinement procedure
Resolution | 24.377 - 1.570 |
R-factor | 0.1874 |
Rwork | 0.187 |
R-free | 0.21130 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.079 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | |
High resolution limit [Å] | 1.570 | 1.570 |
Rmerge | 0.115 | 0.570 |
Number of reflections | 103855 | |
<I/σ(I)> | 16.37 | 2.1 |
Completeness [%] | 99.6 | 94.8 |
Redundancy | 4.5 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 291 | 10% PEG20000, 100 mM sodium citrate, pH 5.0, and 200 mM MgCl2 |