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5DBR

Ca2+ CaM with human cardiac Na+ channel (NaV1.5) inactivation gate

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsBRUKER AXS MICROSTAR
Temperature [K]100
Detector technologyCCD
Collection date2013-07-31
DetectorBruker Platinum 135
Wavelength(s)1.5418
Spacegroup nameP 32 2 1
Unit cell lengths58.086, 58.086, 102.638
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution50.300 - 2.250
R-factor0.2236
Rwork0.220
R-free0.28420
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4djc
RMSD bond length0.018
RMSD bond angle1.913
Data reduction softwarePROTEUM PLUS
Data scaling softwareSCALEPACK
Phasing softwarePHASER (2.5.7)
Refinement softwareREFMAC (5.8.0124)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.3002.300
High resolution limit [Å]2.2502.250
Rmerge0.0900.446
Number of reflections9401
<I/σ(I)>18.44.1
Completeness [%]99.6100
Redundancy15.610.56
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP42980.2M sodium malonate pH 4.0, 20% w/v PEG 3350

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