5D6L
beta2AR-T4L - CIM
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-03-01 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.96867 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 107.260, 170.360, 40.270 |
Unit cell angles | 90.00, 105.67, 90.00 |
Refinement procedure
Resolution | 49.760 - 3.200 |
R-factor | 0.2236 |
Rwork | 0.222 |
R-free | 0.26040 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2rh1 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.915 |
Data reduction software | xia2 |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.760 | 3.280 |
High resolution limit [Å] | 3.200 | 3.200 |
Rmerge | 0.143 | 0.814 |
Number of reflections | 10858 | |
<I/σ(I)> | 1.5 | 1.5 |
Completeness [%] | 94.4 | 96.7 |
Redundancy | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 293 | 30 - 35 % Peg 400, 5 -10 % butanediol, 0.1 - 0.35 mM Na sulphate, 0.1 M Bis-Tris pH 7.0. |