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5D5B

In meso X-ray crystallography structure of the Beta2-adrenergic receptor at 100 K

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X10SA
Synchrotron siteSLS
BeamlineX10SA
Temperature [K]100
Detector technologyPIXEL
Collection date2015-02-18
DetectorDECTRIS PILATUS 6M-F
Wavelength(s)1.03321
Spacegroup nameC 1 2 1
Unit cell lengths107.000, 170.000, 40.500
Unit cell angles90.00, 106.25, 90.00
Refinement procedure
Resolution49.618 - 3.800
R-factor0.2416
Rwork0.240
R-free0.27440
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2rh1
RMSD bond length0.006
RMSD bond angle1.144
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHASER
Refinement softwarePHENIX (1.9_1692)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0003.900
High resolution limit [Å]3.8003.800
Number of reflections6835
<I/σ(I)>3.760.96
Completeness [%]99.698.8
Redundancy6.54.58
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1LIPIDIC CUBIC PHASE29330-35 %(v/v) PEG 400, 0.1-0.2 M Na2SO4, 0.1 M bis-tris propane pH 6.5-7.0 and 5-7 %(v/v) 1,4-butanediol

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