5D0M
Structure of UbE2D2:RNF165:Ub complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2014-11-19 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 |
Unit cell lengths | 62.620, 62.620, 82.250 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.005 - 1.913 |
R-factor | 0.1805 |
Rwork | 0.179 |
R-free | 0.21270 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.080 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 31.310 |
High resolution limit [Å] | 1.910 |
Number of reflections | 24549 |
<I/σ(I)> | 19.3 |
Completeness [%] | 100.0 |
Redundancy | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291.15 | SPG buffer, PEG 1500 |