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5CZ4

Yeast 20S proteasome at 2.3 A resolution

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06SA
Synchrotron siteSLS
BeamlineX06SA
Temperature [K]100
Detector technologyPIXEL
Collection date2014-10-14
DetectorPSI PILATUS 6M
Wavelength(s)1.0
Spacegroup nameP 1 21 1
Unit cell lengths137.020, 300.930, 145.760
Unit cell angles90.00, 113.13, 90.00
Refinement procedure
Resolution15.000 - 2.300
R-factor0.21171
Rwork0.211
R-free0.22838
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1ryp
RMSD bond length0.005
RMSD bond angle0.888
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwareREFMAC
Refinement softwareREFMAC (5.7.0032)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0002.400
High resolution limit [Å]2.3002.300
Rmerge0.0610.479
Number of reflections472928
<I/σ(I)>13.12
Completeness [%]98.792.7
Redundancy3.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.829320 mM MgAC2, 13% MPD, 0.1 M MES

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