5CSZ
CRYSTAL STRUCTURE OF GANTENERUMAB FAB FRAGMENT IN COMPLEX WITH ABETA 1-11
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-12-01 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.999 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 71.137, 66.242, 105.156 |
Unit cell angles | 90.00, 99.09, 90.00 |
Refinement procedure
Resolution | 45.640 - 1.800 |
R-factor | 0.19814 |
Rwork | 0.196 |
R-free | 0.23005 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.236 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0062) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.640 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.558 | |
Number of reflections | 89468 | |
<I/σ(I)> | 5.5 | 1.1 |
Completeness [%] | 99.8 | 99.5 |
Redundancy | 3.7 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 25 % PEG 3350, 0.1M Bis-Tris 6.5, 0.2 M ammonium sulfate |