Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-BM |
| Synchrotron site | APS |
| Beamline | 19-BM |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-10-20 |
| Detector | SBC-3 |
| Wavelength(s) | 0.9792 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 159.931, 134.176, 77.477 |
| Unit cell angles | 90.00, 114.43, 90.00 |
Refinement procedure
| Resolution | 36.800 - 2.380 |
| R-factor | 0.1881 |
| Rwork | 0.185 |
| R-free | 0.23570 |
| Structure solution method | SAD |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.483 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 38.600 | 40.000 | 2.470 |
| High resolution limit [Å] | 2.380 | 5.490 | 2.400 |
| Rmerge | 0.066 | 0.036 | 0.484 |
| Total number of observations | 532616 | ||
| Number of reflections | 58601 | ||
| <I/σ(I)> | 10.6 | ||
| Completeness [%] | 98.2 | 99 | 91.6 |
| Redundancy | 4.6 | 4.6 | 3.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 294 | 0.1 M Tris buffer, 8% isopropanol |
