5CJE

Structure of CYP107L2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	100
Detector technology	CCD
Collection date	2013-07-22
Detector	ADSC QUANTUM 270
Wavelength(s)	0.97952
Spacegroup name	C 1 2 1
Unit cell lengths	110.184, 50.585, 74.638
Unit cell angles	90.00, 98.91, 90.00

Refinement procedure

Resolution	36.870 - 2.500
R-factor	0.17435
Rwork	0.170
R-free	0.25545
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2cd8
RMSD bond length	0.012
RMSD bond angle	1.624
Phasing software	PHASER
Refinement software	REFMAC (5.8.0103)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.540
High resolution limit [Å]	2.500	2.500
Rmerge		0.474
Number of reflections	14255
<I/σ(I)>	30.5	7.8
Completeness [%]	99.2	100
Redundancy	5.3	5.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		287	Sodium Citrate, Imidazole