5CHF
Crystal structure of murine ISG15 in space group P21212
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-04-28 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 57.990, 168.290, 85.350 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.966 - 2.300 |
R-factor | 0.2105 |
Rwork | 0.208 |
R-free | 0.26570 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1z2m |
RMSD bond length | 0.006 |
RMSD bond angle | 1.078 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.400 | |
High resolution limit [Å] | 2.300 | 8.000 | 2.300 |
Rmerge | 0.182 | 0.030 | 1.762 |
Rmeas | 0.197 | 0.033 | 1.919 |
Total number of observations | 267134 | ||
Number of reflections | 37611 | 1001 | 4314 |
<I/σ(I)> | 10.91 | 41.54 | 1.04 |
Completeness [%] | 99.0 | 97.8 | 96.2 |
Redundancy | 7.1 | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | 0.7 M (NH4)2 SO4, 0.06 mM ZnSO4 |