5CB7
Crystallographic structure of human rotavirus K8 VP8* in complex with A-type HBGA
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
| Synchrotron site | Australian Synchrotron |
| Beamline | MX1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-06-08 |
| Detector | ADSC QUANTUM 210r |
| Wavelength(s) | 0.954 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 42.270, 83.190, 47.750 |
| Unit cell angles | 90.00, 94.03, 90.00 |
Refinement procedure
| Resolution | 47.630 - 1.350 |
| R-factor | 0.17142 |
| Rwork | 0.170 |
| R-free | 0.19189 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.400 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 47.640 |
| High resolution limit [Å] | 1.350 |
| Number of reflections | 69208 |
| <I/σ(I)> | 6.3 |
| Completeness [%] | 96.0 |
| Redundancy | 4.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 1.6 M sodium citrate pH 6.5 |
