5CAW
Structure of Pediculus humanus Parkin bound to phospho-ubiquitin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-05-27 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97949 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 49.170, 44.120, 204.531 |
Unit cell angles | 90.00, 92.55, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.060 | 2.740 |
High resolution limit [Å] | 2.620 | 2.620 |
Rmerge | 0.085 | 0.389 |
Number of reflections | 26558 | |
<I/σ(I)> | 6.3 | 2 |
Completeness [%] | 99.6 | 99.6 |
Redundancy | 3 | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 2% (v/v) PEG400, 2 M NH4SO4, 0.1 M HEPES pH 7.5 |