Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX9.6 |
Synchrotron site | SRS |
Beamline | PX9.6 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1996-06-15 |
Detector | MAR scanner 300 mm plate |
Wavelength(s) | 0.88 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 155.116, 120.439, 108.836 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.946 - 2.500 |
R-factor | 0.1856 |
Rwork | 0.183 |
R-free | 0.22490 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.812 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 100.000 |
High resolution limit [Å] | 2.500 |
Rmerge | 0.090 |
Number of reflections | 35633 |
<I/σ(I)> | 7.8 |
Completeness [%] | 99.9 |
Redundancy | 5.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 0.1 M Li2SO4, 50 mM Na Citrate pH5.6, 15% PEG4000 |