5AUY
Crystal structure of DAPK1 in complex with morin.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-11-02 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.837, 62.210, 88.315 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.453 - 2.000 |
R-factor | 0.2088 |
Rwork | 0.207 |
R-free | 0.24930 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.962 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 34.500 |
High resolution limit [Å] | 2.000 |
Number of reflections | 17897 |
<I/σ(I)> | 18.5 |
Completeness [%] | 97.7 |
Redundancy | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 2 M ammonium sulfate, 0.1 M MES |