5APU
Sequence IANKEDKAD inserted between GCN4 adaptors - Structure A9b black
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-04-02 |
Detector | DECTRIS PILATUS |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 26.200, 37.520, 95.000 |
Unit cell angles | 90.00, 92.56, 90.00 |
Refinement procedure
Resolution | 34.890 - 1.350 |
R-factor | 0.16513 |
Rwork | 0.163 |
R-free | 0.19908 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2wpq |
RMSD bond length | 0.005 |
RMSD bond angle | 0.869 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.900 | 1.430 |
High resolution limit [Å] | 1.350 | 1.350 |
Rmerge | 0.030 | 0.670 |
Number of reflections | 39198 | |
<I/σ(I)> | 17.6 | 2.1 |
Completeness [%] | 95.9 | 92.1 |
Redundancy | 3.72 | 3.47 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 2.4 M SODIUM MALONATE PH 5.0 |