5AJI
MscS D67R1 high resolution
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-4 |
| Synchrotron site | ESRF |
| Beamline | ID14-4 |
| Temperature [K] | 100 |
| Collection date | 2013-01-01 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 126.330, 149.090, 173.820 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 68.510 - 2.990 |
| R-factor | 0.2454 |
| Rwork | 0.244 |
| R-free | 0.26331 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4age |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.203 |
| Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 64.000 | 3.070 |
| High resolution limit [Å] | 2.990 | 2.990 |
| Rmerge | 0.082 | 1.002 |
| Number of reflections | 66747 | |
| <I/σ(I)> | 6.7 | 1.1 |
| Completeness [%] | 99.5 | 99.8 |
| Redundancy | 3.3 | 3.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
