5AFJ
alpha7-AChBP in complex with lobeline and fragment 1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-11-10 |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 85.203, 106.477, 140.989 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.383 - 2.200 |
R-factor | 0.1715 |
Rwork | 0.168 |
R-free | 0.23290 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.007 |
RMSD bond angle | 1.178 |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 48.380 |
High resolution limit [Å] | 2.220 |
Rmerge | 0.060 |
Number of reflections | 63044 |
<I/σ(I)> | 12.2 |
Completeness [%] | 98.8 |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |