5AES
Crystal Structure of murine Chronophin (Pyridoxal Phosphate Phosphatase) in Complex with a PNP-derived Inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2013-10-02 |
Detector | RIGAKU IMAGE PLATE |
Spacegroup name | I 2 3 |
Unit cell lengths | 166.810, 166.810, 166.810 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.714 - 2.751 |
R-factor | 0.1923 |
Rwork | 0.190 |
R-free | 0.24660 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4bx3 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.932 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.710 | 2.900 |
High resolution limit [Å] | 2.750 | 2.750 |
Rmerge | 0.100 | 0.950 |
Number of reflections | 20219 | |
<I/σ(I)> | 13 | 1.9 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.3 | 7.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8 | 0.1M IMIDAZOLE (PH 8.0), 0.2M NACL, 1M SODIUM TARTRATE |