5A2I
Crystal structure of scFv-SM3 in complex with APD-SGalNAc-RP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 33.181, 66.006, 90.290 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 90.290 - 1.880 |
R-factor | 0.20748 |
Rwork | 0.206 |
R-free | 0.26131 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1sm3 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.829 |
Data reduction software | XDS |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.980 |
High resolution limit [Å] | 1.880 | 1.880 |
Rmerge | 0.080 | 0.550 |
Number of reflections | 16818 | |
<I/σ(I)> | 10.4 | 2.4 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 6.2 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |