5ZXM
Crystal Structure of GyraseB N-terminal at 1.93A Resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-1 |
Synchrotron site | ESRF |
Beamline | MASSIF-1 |
Temperature [K] | 273 |
Detector technology | PIXEL |
Collection date | 2018-02-09 |
Detector | DECTRIS PILATUS3 2M |
Wavelength(s) | 0.96 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 79.420, 86.530, 135.990 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 73.004 - 1.938 |
R-factor | 0.1824 |
Rwork | 0.181 |
R-free | 0.22550 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ei1 |
Data reduction software | XDS |
Data scaling software | autoPROC |
Phasing software | PHASER |
Refinement software | REFMAC (5.5) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 73.004 | 1.970 |
High resolution limit [Å] | 1.938 | 1.940 |
Rmerge | 0.101 | 0.800 |
Number of reflections | 69892 | 3436 |
<I/σ(I)> | 10.3 | |
Completeness [%] | 99.3 | |
Redundancy | 4.5 | |
CC(1/2) | 0.990 | 0.670 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | PEG 3350, lithium sulfate, ATP, Tris, pH 8.0 |