5YU7
CRYSTAL STRUCTURE OF EXPORTIN-5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-02-02 |
Detector | RAYONIX MX300HE |
Wavelength(s) | 0.9000 |
Spacegroup name | P 64 |
Unit cell lengths | 286.163, 286.163, 59.349 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.304 - 3.301 |
R-factor | 0.2011 |
Rwork | 0.200 |
R-free | 0.22920 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3a6p |
RMSD bond length | 0.002 |
RMSD bond angle | 0.442 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.360 |
High resolution limit [Å] | 3.300 | 3.300 |
Rmerge | 0.068 | 0.845 |
Number of reflections | 42325 | 2056 |
<I/σ(I)> | 28 | 1.9 |
Completeness [%] | 99.5 | 100 |
Redundancy | 4.7 | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 283 | PEG3350, Tacsimate, MPD, MgCl2, DTT |