5YEH
Crystal structure of CTCF ZFs4-8-eCBS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-11-07 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9785 |
Spacegroup name | P 1 |
Unit cell lengths | 45.845, 54.876, 66.938 |
Unit cell angles | 81.17, 80.11, 79.72 |
Refinement procedure
Resolution | 32.706 - 2.328 |
R-factor | 0.2243 |
Rwork | 0.222 |
R-free | 0.26950 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5yeg |
RMSD bond length | 0.010 |
RMSD bond angle | 1.208 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.710 | 2.380 |
High resolution limit [Å] | 2.330 | 2.340 |
Rmerge | 0.073 | 0.660 |
Rpim | 0.034 | 0.306 |
Number of reflections | 25836 | |
<I/σ(I)> | 20.2 | 2.54 |
Completeness [%] | 96.5 | 97.4 |
Redundancy | 5.4 | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 289 | 0.1 M Bis-tris pH 5.6-6.0, 0.2 M Sodium chloride and 17-24% PEG 3350 |