5WC9
Human Pit-1 and 4xCATT DNA complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 93.15 |
Detector technology | IMAGE PLATE |
Collection date | 2017-04-28 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.541870 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 66.415, 97.518, 85.093 |
Unit cell angles | 90.00, 93.65, 90.00 |
Refinement procedure
Resolution | 47.200 - 3.150 |
R-factor | 0.2327 |
Rwork | 0.231 |
R-free | 0.27720 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1au7 |
RMSD bond length | 0.005 |
RMSD bond angle | 0.587 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.200 | 3.263 |
High resolution limit [Å] | 3.150 | 3.150 |
Rmerge | 0.224 | 0.532 |
Rpim | 0.076 | 0.281 |
Number of reflections | 18198 | 1681 |
<I/σ(I)> | 10.57 | 2.24 |
Completeness [%] | 95.9 | 87.13 |
Redundancy | 9.2 | 3.9 |
CC(1/2) | 0.990 | 0.989 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.1 M MES pH 6.5, 17.5% (w/v) PEG 6000, 5%(v/v) MPD |