5TGL

A MODEL FOR INTERFACIAL ACTIVATION IN LIPASES FROM THE STRUCTURE OF A FUNGAL LIPASE-INHIBITOR COMPLEX

Experimental procedure

Spacegroup name	C 2 2 21
Unit cell lengths	48.300, 93.900, 122.100
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	? - 3.000
R-factor	0.185
Phasing software	X-PLOR
Refinement software	PROLSQ

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	5.440 *
High resolution limit [Å]	3.000 *	3.000 *
Rmerge	0.079 *	0.186 *
Number of reflections	5892 *	965 *
Completeness [%]	87.3 *	27.1 *
Redundancy	6.6 *	2.0 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	20 (mg/ml)
2	1	reservoir	PEG600	7-10 (%(v/v))