5T8R
Crystal structure of human BAZ2A PHD zinc finger in complex with unmodified H3 10-mer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-10-02 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9762 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 72.607, 72.607, 99.431 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.620 - 2.400 |
R-factor | 0.1877 |
Rwork | 0.185 |
R-free | 0.23530 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4qf2 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.510 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.15) |
Refinement software | REFMAC (5.8.0131) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 45.620 | 45.620 | 2.490 |
High resolution limit [Å] | 2.400 | 8.980 | 2.400 |
Rmerge | 0.113 | 0.057 | 0.782 |
Number of reflections | 10901 | ||
<I/σ(I)> | 9.3 | ||
Completeness [%] | 99.6 | 95.7 | 100 |
Redundancy | 5.4 | 4.5 | 5.8 |
CC(1/2) | 0.994 | 0.999 | 0.718 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 291 | 2.2 M Na/K phosphate |