5O23
Crystal structure of WNK3 kinase domain in a monophosphorylated apo state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-06-27 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.976 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 124.020, 124.020, 107.370 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 75.930 - 2.250 |
R-factor | 0.2068 |
Rwork | 0.205 |
R-free | 0.23870 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.001 |
RMSD bond angle | 0.432 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 75.930 |
High resolution limit [Å] | 2.250 |
Number of reflections | 45616 |
<I/σ(I)> | 24.8 |
Completeness [%] | 99.9 |
Redundancy | 10.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 30% PEG Smear Medium, 0.2 M lithium sulfate, 0.1 M ADA pH 6.5 |