5N8A
Structure of RPA70N in complex with PrimPol (fragment 480-560)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-11-30 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.91407 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 38.050, 53.490, 53.900 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 16.247 - 1.280 |
R-factor | 0.1549 |
Rwork | 0.154 |
R-free | 0.17850 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ipc |
RMSD bond length | 0.007 |
RMSD bond angle | 0.912 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER (2.5.6) |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 16.247 | 16.247 | 1.310 |
High resolution limit [Å] | 1.280 | 5.720 | 1.280 |
Rmerge | 0.043 | 0.019 | 0.604 |
Rmeas | 0.047 | 0.020 | 0.700 |
Total number of observations | 351864 | ||
Number of reflections | 351864 | 595 | 4028 |
<I/σ(I)> | 20.01 | 73.95 | 1.87 |
Completeness [%] | 99.7 | 95 | 97.7 |
Redundancy | 6.431 | 6.931 | 3.845 |
CC(1/2) | 1.000 | 1.000 | 0.677 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 293.15 | 0.2M imidazole malate, 30% w/v PEG 4000 |