5MWB
Human Notch-2 EGF11-13
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-04-19 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 20.160, 49.790, 125.500 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.003 - 1.860 |
R-factor | 0.2298 |
Rwork | 0.228 |
R-free | 0.26360 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vj3 |
RMSD bond length | 0.021 |
RMSD bond angle | 0.550 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.800 | 1.910 |
High resolution limit [Å] | 1.860 | 1.860 |
Rmerge | 0.077 | 1.067 |
Number of reflections | 11247 | |
<I/σ(I)> | 11.2 | 1.3 |
Completeness [%] | 99.5 | 99.3 |
Redundancy | 5.2 | 5.1 |
CC(1/2) | 0.998 | 0.524 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.5 | 293 | PEG 8000, Sodium acetate, Sodium cacodylate |