5MUJ
BT0996 RGII Chain B Complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-05-15 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.976 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 49.460, 80.000, 50.810 |
| Unit cell angles | 90.00, 114.94, 90.00 |
Refinement procedure
| Resolution | 44.850 - 1.370 |
| R-factor | 0.20077 |
| Rwork | 0.198 |
| R-free | 0.25181 |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.709 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 44.850 |
| High resolution limit [Å] | 1.370 |
| Number of reflections | 74740 |
| <I/σ(I)> | 1.4 |
| Completeness [%] | 99.0 |
| Redundancy | 3.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 20% (w/v) PEG 3350 and 0.2 M Lithium Acetate |
