Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-01-01 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 1.00002 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 57.850, 57.850, 366.480 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 57.000 - 3.400 |
| R-factor | 0.2584 |
| Rwork | 0.255 |
| R-free | 0.29590 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4OE8 |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.850 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 57.000 | 3.500 |
| High resolution limit [Å] | 3.400 | 3.400 |
| Rmeas | 0.116 | 0.921 |
| Number of reflections | 9551 | |
| <I/σ(I)> | 20.7 | 5.2 |
| Completeness [%] | 99.8 | 100 |
| Redundancy | 22.29 | 23.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.3 | 294 | 0.2M POTASSIUM FORMATE, 20.75% W/V PEG 3350, PH 7.3 |
