5LX3
CRYSTAL STRUCTURE OF VISFATIN IN COMPLEX WITH SAR154782.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-01-26 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.987 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 61.510, 107.130, 83.590 |
Unit cell angles | 90.00, 96.69, 90.00 |
Refinement procedure
Resolution | 46.930 - 2.100 |
Rwork | 0.172 |
R-free | 0.21100 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | BUSTER-TNT |
Refinement software | BUSTER-TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.930 | 2.230 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.139 | 0.385 |
Number of reflections | 62781 | |
<I/σ(I)> | 11.3 | 3 |
Completeness [%] | 100.0 | 99.8 |
Redundancy | 3.4 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 292 | Tris 100mM - PEG8000 16% - pH8,5 |