5LSP
107_A07 Fab in complex with fragment of the Met receptor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-05-29 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.91376 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 71.880, 82.279, 267.304 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.942 - 2.605 |
R-factor | 0.2171 |
Rwork | 0.215 |
R-free | 0.25650 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 0.999 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX (1.9_1692) |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 48.950 | 48.950 | 2.740 |
High resolution limit [Å] | 2.600 | 8.230 | 2.600 |
Rmerge | 0.110 | 0.032 | 0.883 |
Number of reflections | 49099 | ||
<I/σ(I)> | 11.7 | 33.6 | 2 |
Completeness [%] | 99.0 | 99 | 95.8 |
Redundancy | 5.5 | 4.9 | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | 10% PEG 20,000, 20% PEG 550-MME, 0.1M Trizma/Bicine pH 8.5, 0.03M magnesium chloride, 0.03M calcium chloride |