5L9R
HIF prolyl hydroxylase 2 (PHD2/ EGLN1) in complex with N-oxalylglycine (NOG)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-09-17 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9795 |
Spacegroup name | P 41 |
Unit cell lengths | 71.233, 71.233, 48.245 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.950 - 1.810 |
R-factor | 0.1577 |
Rwork | 0.156 |
R-free | 0.18800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4bqy |
RMSD bond length | 0.005 |
RMSD bond angle | 0.776 |
Data reduction software | HKL-2000 (706E) |
Data scaling software | HKL-2000 (706E) |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.945 | 1.870 |
High resolution limit [Å] | 1.806 | 1.810 |
Rmerge | 0.106 | 0.977 |
Number of reflections | 22342 | |
<I/σ(I)> | 18.372 | 1.875 |
Completeness [%] | 99.9 | 99.1 |
Redundancy | 7.3 | 6.7 |
CC(1/2) | 0.995 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | 0.1 M HEPES-Na pH 7.5, 2% v/v Polyethylene glycol 400, 2.0 M ammonium sulfate |