5IT1
Streptomyces peucetius CYP105P2 complex with biphenyl compound
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
| Synchrotron site | PAL/PLS |
| Beamline | 7A (6B, 6C1) |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2015-02-25 |
| Detector | ADSC QUANTUM 270 |
| Wavelength(s) | 0.97934 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 123.023, 122.941, 193.287 |
| Unit cell angles | 90.00, 90.03, 90.00 |
Refinement procedure
| Resolution | 50.000 - 2.100 |
| R-factor | 0.20247 |
| Rwork | 0.200 |
| R-free | 0.24297 |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.966 |
| Data scaling software | HKL-2000 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.100 |
| Number of reflections | 165620 |
| <I/σ(I)> | 39.3 |
| Completeness [%] | 99.5 |
| Redundancy | 6.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 0.1 M Bis-Tris Propane, 0.2 M DL-Malic acid |
