5GID
Crystal structure of VDR in complex with DLAM-4 (C2 form)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL41XU |
| Synchrotron site | SPring-8 |
| Beamline | BL41XU |
| Temperature [K] | 90 |
| Detector technology | CCD |
| Collection date | 2014-06-14 |
| Detector | MAR CCD 130 mm |
| Wavelength(s) | 1.0000 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 154.510, 42.345, 42.320 |
| Unit cell angles | 90.00, 96.46, 90.00 |
Refinement procedure
| Resolution | 40.821 - 2.151 |
| R-factor | 0.202 |
| Rwork | 0.199 |
| R-free | 0.23330 |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.879 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | MOLREP |
| Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 41.000 |
| High resolution limit [Å] | 2.150 |
| Number of reflections | 14860 |
| <I/σ(I)> | 13.33 |
| Completeness [%] | 99.0 |
| Redundancy | 3.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1M Tris-HCl, PEG 8000, NaCl |
