5GIC

Crystal structure of VDR in complex with DLAM-2P

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE AR-NE3A
Synchrotron site	Photon Factory
Beamline	AR-NE3A
Temperature [K]	90
Detector technology	CCD
Collection date	2013-01-31
Detector	MAR CCD 130 mm
Wavelength(s)	1.0000
Spacegroup name	C 1 2 1
Unit cell lengths	154.315, 42.444, 42.106
Unit cell angles	90.00, 96.53, 90.00

Refinement procedure

Resolution	30.000 - 2.352
R-factor	0.2202
Rwork	0.217
R-free	0.25060
RMSD bond length	0.004
RMSD bond angle	0.922
Data reduction software	XDS
Data scaling software	XDS
Phasing software	MOLREP
Refinement software	PHENIX ((1.10.1_2155))

Data quality characteristics

	Overall
Low resolution limit [Å]	30.000
High resolution limit [Å]	2.350
Number of reflections	11424
<I/σ(I)>	10.3
Completeness [%]	99.0
Redundancy	3.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	0.1M Tris-HCl, PEG 8000, NaCl