5G44
Ligand complex of RORg LBD
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | PILATUS |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 61.840, 61.840, 156.430 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 48.510 - 1.840 |
| R-factor | 0.1901 |
| Rwork | 0.188 |
| R-free | 0.22930 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.010 |
| RMSD bond angle | 0.950 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Refinement software | BUSTER (2.11.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.510 | 1.900 |
| High resolution limit [Å] | 1.840 | 1.840 |
| Rmerge | 0.120 | |
| Number of reflections | 27281 | |
| <I/σ(I)> | 14.6 | 1.8 |
| Completeness [%] | 99.9 | 99.9 |
| Redundancy | 12.4 | 12.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
