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5FPU

Crystal structure of human JARID1B in complex with GSKJ1

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04
Synchrotron siteDiamond
BeamlineI04
Temperature [K]100
Detector technologyPIXEL
Collection date2015-05-06
DetectorDECTRIS PILATUS 6M
Spacegroup nameP 65 2 2
Unit cell lengths141.660, 141.660, 151.980
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution64.601 - 2.240
R-factor0.1911
Rwork0.190
R-free0.22110
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)5a1f
RMSD bond length0.002
RMSD bond angle0.719
Data reduction softwareXDS
Data scaling softwareSCALA
Phasing softwareMOLREP
Refinement softwarePHENIX ((PHENIX.REFINE))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]95.4602.300
High resolution limit [Å]2.2402.240
Rmerge0.0900.090
Number of reflections43823
<I/σ(I)>4.824.9
Completeness [%]100.0100
Redundancy20.219.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
180.1M HEPES PH 8.0, 0.8M POTASSIUM PHOSPHATE-DIBASIC, 0.8M SODIUM PHOSPHATE MONOBASIC

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